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This issue contains 27 papers from The American Ceramic Society's 40th International Conference on Advanced Ceramics and Composites, held in Daytona Beach, Florida, January 24-29, 2016. This issue includes papers presented in the following Symposia and Focused Sessions: Symposium 2 - Advanced Ceramic Coatings for Structural, Environmental, and Functional Applications; Symposium 10 - Virtual Materials (Computational) Design and Ceramic Genome; Symposium 11 - Advanced Materials and Innovative Processing Ideas for the Industrial Root Technology; Symposium 12 - Materials for Extreme Environments: Ultrahigh Temperature Ceramics; and Emerging Technologies Symposium-Carbon Nanostructures; and Focused Session 1 - Geopolymers and Chemically Bonded Ceramics.
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Edited by Waltraud M. Kriven Jingyang WangYanchun ZhouDongming ZhuGustavo Costa
Volume Editors Manabu Fukushima Andrew Gyekenyesi
Copyright © 2017 by The American Ceramic Society. All rights reserved.
Published by John Wiley & Sons, Inc., Hoboken, New Jersey.
Published simultaneously in Canada.
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ISBN: 978-1-119-32178-1 ISSN: 0196-6219
Preface
Introduction
Geopolymers
Durability Performance of Alkali-Activated Metakaolin, Slag, Fly Ash, and Hybrids
Abstract
Introduction
Experimental Procedures
Results & Discussion
Summary and Conclusion
Acknowledgements
References
MICA Platelet-Reinforced Geopolymer Composites
Abstract
Introduction
Experimental
Results
Conclusion
Acknowledgements
References
Influence of Mix Design Parameters on Geopolymer Mechanical Properties and Microstructure
Abstract
Introduction
Experimental Investigation
Experimental Results and Discussion
Conclusions
Acknowledgements
References
Thermal Performance of Metakaolin-Based Geopolymers: Volume Stability and Residual Mechanical Properties
Abstract
Introduction
Experimental Program
Experimental Results and Discussion
Conclusions
Acknowledgements
References
Effect of Phyllosilicate Type on the Microstructure and Properties of Kaolin-Based Ceramic Tapes
Abstract
Introduction
Materials
Methods
Results and Discussion
Conclusion and Prospects
Acknowledgement
References
Effect of Alkali Cations on the Polycondensation Reaction
Abstract
Introduction
Experimental
Results
Discussion
Conclusions
References
Development of a Mold for Thermoplastics Based on a Phosphate Cement
Abstract
Introduction
Experimental Work
Results and Discussion
Proof of Concept
Conclusions
References
Properties of Cork Particle Reinforced Sodium Geopolymer Composites
Abstract
Introduction
Experimental Procedure
Results and Discussion
Conclusion
Acknowledgement
References
The Role of Alkaline Earth Ions in Geopolymer Binder Formation
Abstract
Introduction
Experimental Part
Results and Discussion
Conclusion
References
Investigations of the Thermally Induced Hydrogen Release of NaBH
4
, NH
3
BH
3
and Their Geopolymer Composites
Abstract
Introduction
Experimental
Results and Discussion
Conclusion
References
IR-Spectroscopic Investigation of Geopolymer and CSH-Phase Stability on Heating Temperature in Post-Fired Building Materials
Abstract
Introduction
Experimental
Results and Discussion
Conclusions
References
Mixed Alkali Regional Metakaolin-based Geopolymer
Abstract
Introduction
Experimental Procedures
Results and Discussion
Conclusions
Acknowledgements
References
Bamboo-Geopolymer Composite: A Preliminary Study
Abstract
Introduction
Materials and Methods
Results and Discussion
Conclusions
Acknowledgements
References
Metakaolin-Based Geopolymer Cements from Commercial Sodium Waterglass and Sodium Waterglass from Rice Husk Ash: A Comparative Study
Abstract
Introduction
Materials and Experimental Methods
Results and Discussion
Conclusion
Acknowledgments
References
Recycling of Grog by Addition into Heavy Clay Ceramic Manufacturing
Abstract
Introduction
Materials and Methods
Results and Discussion
Conclusions
Acknowledgements
References
Virtual Materials Design and Ceramic Genome
Q-State Monte Carlo Simulations of Magnetic Anisotropy Applied to Paramagnetic and Diamagnetic Materials
Abstract
Introduction
The Model
Results
Conclusions
Acknowledgments
References
First Principles Study of Defect Formation in Bulk B
6
O
Abstract
Introduction
Computational Details
Results and Discussion
Conclusions
Acknowledgements
References
Modeling of Damage in an MMC with Lamellar Microstructure
Abstract
Introduction
Materials and Experimental
Analytical Modelling
FE Modelling
Results and Discussion
Conclusions and Outlook
Acknowledgement
References
Micro-Computed Tomography Image based Thermo-Elastic Properties Studies of Freeze-Cast MMC
Abstract
Introduction
Materials and Experimental
Material Modelling and Discussion
Conclusions
Acknowledgement
References
Materials for Extreme Environments
Densification and Phase Evolution of SHS Derived Ti
2
AlN Active Precursor Powders During Hot Pressing Processes
Abstract
Introduction
Preparation
Results and Discussion
Conclusions
Acknowledgments
References
Max Phase Materials for Nuclear Applications
Abstract
Introduction
Experimental
Results and Discussion
Conclusions
Acknowledgements
References
Analysis of Dynamic Young's Modulus and Damping Behavior of ZrB
2
-SiC Composites by the Impulse Excitation Technique
Abstract
Introduction
Experimental Methods
Results and Discussion
Conclusions
Acknowledgements
References
Advanced Ceramic Coatings
Study of Effect of Hafnium Addition on Oxidation Resistance of βNiAl Coatings Prepared by an in-situ Chemical Vapour Deposition Method
Abstract
Introduction
Experimental
Results
TGO
Discussion
Conclusions
Acknowledgments
References
Mass Transfer Mechanism in Mullite Under Oxygen Potential Gradients at High Temperatures
Abstract
Introduction
Experimental
Results and Discussion
Conclusions
Acknowledgements
References
Emerging Technologies— Carbon Nanostructures
SnO
2
-Reduced Graphene Oxide Nanocomposite for Ethanol Sensing at Room Temperature
Abstract
Introduction
Experimental
Results and Discussion
Conclusions
Acknowledgements
References
Author Index
EULA
Chapter 1
Table 1
Chemical composition of solid materials (wt%)
Table 2
Mixture proportion of alkali-activated metakaolin (AAMK), fly ash (AAB), slag (AAH) and hybrids in weight ratio
Table 3
Mixture proportions of OPC, modified-OPC, and AAC mortar prisms
Chapter 2
Table 1
Thermal conductivity of geopolymer composites as a function of mica content
Chapter 3
Table 1
Chemical composition of Meta Max (Metakaolin from BASF Co., Germany)
Table 2
Mix proportion of metakaolin geopolymers
Chapter 4
Table I
Chemical composition (by weight) of MetaMax (Metakaolin from BASF)
Table II
Mix proportion of metakaolin geopolymers
Chapter 5
Table 1
Chemical compositions (wt.%) of the different clays
Table 2
Characteristic sizes and other physical parameters of kaolin, talc and palygorskite
Chapter 6
Table 1
Physical and chemical feature of silicate solutions before and after the addition of hydroxide pellets
Table 2
Physical and chemical features of metakaolin
Chapter 9
Table 1
The chemical compositions of the various geopolymer binders with A= Ca, Mg or Sr
Chapter 11
Table 1
Compressive strength of samples AAMK and AAH
Chapter 12
Table 1
Chemical composition of KA and MKA by XRF
Table 2
Average compressive strength of 25x50-mm tested samples with Weibull parameters
Table 3
Average 4-point flexural strength of 30x12-mm tested samples with Weibull parameters
Chapter 13
Table 1
Third-point loading flexural strength results and Weibull parameters
Chapter 14
Table 1
Chemical composition of Dibo, RHA and PRHA in mass percent
Table 2
Compressive strength of geopolymer cements (MPa), the values of main band on the IR spectra of geopolymer cements (cm
-1
) and mass loss (%)
Chapter 15
Table I
Chemical composition of the raw materials (wt %)
Chapter 17
Table I
Change in cohesive energy (Δ CE) and Percent Unit Cell Volume Contraction for single and multi-atom 1
st
, 2
nd
, 3
rd
, and 4
th
nearest neighboring vacancies in B
6
O. See Figure 2 for site notation. Note: B
p-intericosahedral
is the inter-icosahedral link to a polar boron site from nearest neighboring boron icosahedra and Ochain is the nearest neighboring oxygen to O1
Chapter 18
Table 1
Chapter 20
Table I
Phase composition of Ti
2
AlN SHS synthesis products
Table II
Phase evolution of hot-pressed SHS derived Ti
2
AlN powders obtained as a result of synthesis of 3Al + 4 Ti
3
Al under 1.5 atm. nitrogen pressure [wt.%]
Table III
Phase evolution of hot-pressed SHS derived Ti
2
AlN powders obtained as a result of synthesis of 2Al + 4 Ti
3
Al under 1.5 atm. nitrogen pressure [wt.%]
Table IV
Phase evolution of hot-pressed SHS derived Ti
2
AlN powders obtained as a result of synthesis of 2Al + 4 Ti
3
Al under 5 atm. nitrogen pressure [wt.%]
Table V
Apparent densities of hot-pressed Ti
2
AlN materials [g/cm
3
]
Chapter 21
Table 1
The investigated Zr-Al-C starting compositions, sintering temperatures and identified phase assemblies. The majority phases are indicated in bold. The composition of the Zr
4
AlC
3
, Zr
3
AlC
2
and Zr
2
AlC nominal stoichiometries are presented in the bottom three rows
Table 2
Experimental lattice parameters for the Zr
2
AlC and Zr
3
AlC
2
compounds, as obtained by Rietveld refinement of the XRD spectra
Table 3
Mechanical properties of Nb
4
AlC
3
and (Nb
0.85
,Zr
0.15
)
4
AlC
3
at room temperature
Chapter 22
Table I
Mechanical properties of ZrB
2
-SiC composites
Table II
Coefficients A
0
, A
1
and A
2
of (3) with T in (°C) and E in (GPa), obtained from the best fits to the experimental data shown in Figure 4. In the last column, the goodness of the fit is given by the coefficient of determination R
2
Table III
Damping peaks and temperature for each ZrB
2
-SiC composite
Chapter 23
Table 1
show an averaged EDS point analysis taken at different locations of coating cross-sections as-deposited condition
Cover
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This CESP proceedings issue contains a total of 25 contributions from select symposia held during the 40th International Conference on Advanced Ceramics and Composites (ICACC), in Daytona Beach, FL, January 24–29, 2016.
The wide range of topics in this issue were presented in the following Symposia and Focused Sessions:
Symposium 2—Advanced Ceramic Coatings for Structural, Environmental, and Functional Applications
Symposium 10—Virtual Materials (Computational) Design and Ceramic Genome
Symposium 12—Materials for Extreme Environments: Ultrahigh Temperature Ceramics and Nanolaminated Ternary Carbides and Nitrides
Focused Session 1—Geopolymers and Chemically Bonded Ceramics
Emerging Technologies Symposium on Carbon Nanostructures
The editors wish to thank the symposium organizers for their time and efforts, the authors and presenters for their contributions; and the reviewers for their valuable comments and suggestions. In addition, acknowledgments are due to the officers of the Engineering Ceramics Division of The American Ceramic Society and the 2016 ICACC program chair, Andrew Gyekenyesi, for their support. It is the hope that this volume becomes a useful resource for academic, governmental, and industrial efforts.
WALTRAUD M. KRIVEN, University of Illinois at Urbana-Champaign, USA JINGYANG WANG, Institute of Metal Research, Chinese Academy of Sciences, China YANCHUN ZHOU, Aerospace Research Institute of Material & Processing Technology, China
DONGMING ZHU, NASA Glenn Research Center, USA GUSTAVO COSTA, NASA Glenn Research Center, USA
This collected proceedings consists of 104 papers that were submitted and approved for the proceedings of the 40th International Conference on Advanced Ceramics and Composites (ICACC), held January 24–29, 2016 in Daytona Beach, Florida. ICACC is the most prominent international meeting in the area of advanced structural, functional, and nanoscopic ceramics, composites, and other emerging ceramic materials and technologies. This prestigious conference has been organized by the Engineering Ceramics Division (ECD) of The American Ceramic Society (ACerS) since 1977. This year's meeting continued the tradition and added a few grand celebrations to mark its 40th year.
The 40th ICACC hosted more than 1,100 attendees from 42 countries that gave over 900 presentations. The topics ranged from ceramic nanomaterials to structural reliability of ceramic components, which demonstrated the linkage between materials science developments at the atomic level and macro level structural applications. Papers addressed material, model, and component development and investigated the interrelations between the processing, properties, and microstructure of ceramic materials.
The 2016 conference was organized into the following 17 symposia and 5 Focused Sessions:
Symposium 1
Mechanical Behavior and Performance of Ceramics and Composites
Symposium 2
Advanced Ceramic Coatings for Structural, Environmental, and Functional Applications
Symposium 3
13th International Symposium on Solid Oxide Fuel Cells (SOFC): Materials, Science, and Technology
Symposium 4
Armor Ceramics: Challenges and New Developments
Symposium 5
Next Generation Bioceramics and Biocomposites
Symposium 6
Advanced Materials and Technologies for Direct Thermal Energy Conversion and Rechargeable Energy Storage
Symposium 7
10th International Symposium on Nanostructured Materials: Functional Nanomaterials and Thin Films for Sustainable Energy Harvesting, Environmental and Health Applications
Symposium 8
10th International Symposium on Advanced Processing & Manufacturing Technologies for Structural & Multifunctional Materials and Systems
Symposium 9
Porous Ceramics: Novel Developments and Applications
Symposium 10
Virtual Materials (Computational) Design and Ceramic Genome
Symposium 11
Advanced Materials and Innovative Processing ideas for the Production Root Technology
Symposium 11
Materials for Extreme Environments: Ultrahigh Temperature Ceramics (UHTCs) and Nano-laminated
Symposium 12
Ternary Carbides and Nitrides (MAX Phases)
Symposium 13
Advanced Materials for Sustainable Nuclear Fission and Fusion Energy
Symposium 14
Crystalline Materials for Electrical, Optical and Medical Applications
Focused Session 1
Geopolymers, Chemically Bonded Ceramics, Eco-friendly and Sustainable Materials
Focused Session 2
Advanced Ceramic Materials and Processing for Photonics and Energy
Focused Session 3
Materials Diagnostics and Structural Health Monitoring of Ceramic Components and Systems
Focused Session 4
Additive Manufacturing and 3D Printing Technologies
Focused Session 5
Field Assisted Sintering and Related Phenomena at High Temperatures
Focused Session 6
Hybrid Materials and Processing Technologies
Focused Session 7
40th Jubilee Symposium: Engineered Ceramics'Current Status and Future Prospects
Special Symposium
5th Global Young Investigators Forum
Special Symposium
Emerging Technologies Symposium: Carbon Nanostructures and 2D Materials and Composites
The proceedings papers from this conference are published in the below seven issues of the 2016 CESP; Volume 37, Issues 2–7, as listed below.
Mechanical Properties and Performance of Engineering Ceramics and Composites XI, CESP Volume 37, Issue 2 (includes papers from Symposium 1)
Advances in Solid Oxide Fuel Cells and Electronic Ceramics II, CESP Volume 37, Issue 3 (includes papers from Symposia 3 and 14)
Advances in Ceramic Armor, Bioceramics, and Porous Materials, CESP Volume 37, Issue 4 (includes papers from Symposia 4, 5, and 9)
Advanced Processing and Manufacturing Technologies for Nanostructured and Multifunctional Materials III, CESP Volume 37, Issue 5 (includes papers from Symposia 8 and 11 and Focused Sessions 4 and 5)
Ceramic Materials for Energy Applications VI, CESP Volume 37, Issue 6 (includes papers from Symposia 6 and 13 and Focused Session 2)
Developments in Strategic Materials II, CESP Volume 37, Issue 7 (includes papers from Symposia 2, 10, 12, Focused Sessions 1, and the Special Symposia on Carbon).
The organization of the Daytona Beach meeting and the publication of these proceedings were possible thanks to the professional staff of ACerS and the tireless dedication of many ECD members. We would especially like to express our sincere thanks to the symposia organizers, session chairs, presenters and conference attendees, for their efforts and enthusiastic participation in the vibrant and cutting-edge conference.
ACerS and the ECD invite you to attend the 41st International Conference on Advanced Ceramics and Composites (http://www.ceramics.org/icacc2017) January 23-28, 2017 in Daytona Beach, Florida.
To purchase additional CESP issues as well as other ceramic publications, visit the ACerS-Wiley Publications home page at www.wiley.com/go/ceramics.
MANABU FUKUSHIMA, National Institute of Advanced Industrial Science and Technology (AIST), JapanANDREW GYEKENYESI, Ohio Aerospace Institute/NASA Glenn Research Center, USA
Volume Editors August 2016