Applications and Metrology at Nanometer Scale 1 - Pierre-Richard Dahoo - E-Book

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Pierre-Richard Dahoo

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Beschreibung

To develop innovations in quantum engineering and nanosystems, designers need to adopt the expertise that has been developed in research laboratories. This requires a thorough understanding of the experimental measurement techniques and theoretical models, based on the principles of quantum mechanics. This book presents experimental methods enabling the development and characterization of materials at the nanometer scale, based on practical engineering cases, such as 5G and the interference of polarized light when applied for electromagnetic waves. Using the example of electromechanical, multi-physical coupling in piezoelectric systems, smart materials technology is discussed, with an emphasis on scale reduction and mechanical engineering applications. Statistical analysis methods are presented in terms of their usefulness in systems engineering for experimentation, characterization or design, since safety factors and the most advanced reliability calculation techniques are included from the outset. This book provides valuable support for teachers and researchers but is also intended for engineering students, working engineers and Master s students.

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Table of Contents

Cover

Title page

Copyright

Preface

Introduction

1 Nanometer Scale

1.1. Introduction

1.2. Sample elaboration

1.3. Characterization of samples

1.4. Conclusion

1.5. Appendix: light ray propagation

2 Statistical Tools to Reduce the Effect of Design Uncertainties

2.1. Introduction

2.2. Review of fundamental definitions in probability theory

2.3. Random process and random field

2.4. Mathematical formulation of the model

2.5. Reliability-based approach

2.6. Design of experiments method

2.7. Set-based approach

2.8. Analysis in terms of main components

2.9. Applications

2.10. Conclusion

3 Electromagnetic Waves and Their Applications

3.1. Introduction

3.2. Characteristics of the energy carried by an electromagnetic wave

3.3. The energy of a plane monochromatic electromagnetic wave

3.4. Rectangular waveguide as a high-pass frequency filter

3.5. Characteristics of microwave antennas

3.6. Characteristics of networks of microwave antennas

4 Smart Materials

4.1. Introduction

4.2. Smart systems and materials

4.3. Thermodynamics of couplings in active materials

4.4. Exercises on the application of active materials

4.5. Appendix: crystal symmetry

Appendix: Propagation of a Light Ray

References

Index

End User License Agreement

List of Tables

Chapter 2

Table 2.1.

Parameters of the mass–spring–shock absorber system model

Chapter 4

Table 4.1.

Smart materials for sensors and actuators

Table 4.2.

Correspondence for contracting indices C

iklm

to C

ik

Table 4.3.

Correspondence for contracting indices C

iklm

to C

ik

Table 4.4.

Fundamental laws for linear electromagnetic media

Table 4.5.

Correspondence for contracting the indices from d

ikl

to d

ik

Table 4.6.

Piezoelectric effect in tensor and matrix notation

Table 4.7.

Orders of magnitude of the characteristics of some active materials

Table 4.8. The point groups of 32 classes of symmetry and the equivalence betwee...

Table 4.9.

Schoenflies and Hermann–Mauguin notation

Guide

Cover

Title page

Copyright

Preface

Introduction

Begin Reading

Appendix

References

Index

End User License Agreement

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Reliability of Multiphysical Systems Set

coordinated by

Abdelkhalak El Hami

Volume 9

Applications and Metrology at Nanometer Scale 1

Smart Materials, Electromagnetic Waves and Uncertainties

Pierre-Richard Dahoo

Philippe Pougnet

Abdelkhalak El Hami

First published 2021 in Great Britain and the United States by ISTE Ltd and John Wiley & Sons, Inc.

Apart from any fair dealing for the purposes of research or private study, or criticism or review, as permitted under the Copyright, Designs and Patents Act 1988, this publication may only be reproduced, stored or transmitted, in any form or by any means, with the prior permission in writing of the publishers, or in the case of reprographic reproduction in accordance with the terms and licenses issued by the CLA. Enquiries concerning reproduction outside these terms should be sent to the publishers at the undermentioned address:

ISTE Ltd

27-37 St George’s Road

London SW19 4EU

UK

www.iste.co.uk

John Wiley & Sons, Inc.

111 River Street

Hoboken, NJ 07030

USA

www.wiley.com

© ISTE Ltd 2021

The rights of Pierre-Richard Dahoo, Philippe Pougnet and Abdelkhalak El Hami to be identified as the authors of this work have been asserted by them in accordance with the Copyright, Designs and Patents Act 1988.

Library of Congress Control Number: 2020946679

British Library Cataloguing-in-Publication Data

A CIP record for this book is available from the British Library

ISBN 978-1-78630-640-1

Preface

The various actions taken worldwide in support of sustainable development and greenhouse gas emission control have led to increasingly restrictive regulations. Manufacturers in the automotive field have thus developed innovative mechatronic systems, enabling various vehicle functions to go electric. Confronted with the globalization of exchanges that has generated stronger competition and a surge of new product performances, companies in the sector of embedded mechatronic systems are developing new products at an increasingly faster rate.

In other domains, to achieve volume or mass reduction or curb energy dissipation, manufacturers of mechatronic systems are developing new assembly methods based on multimaterials (e.g. composite materials, hybrids) or on innovative nanomaterials (e.g. carbon nanotubes). Modeling is essential to reduce product development cost, shrink time to market, understand failure mechanisms occurring in the operating conditions and optimize design before launching production. The reliability-based design optimization (RBDO) method is a modeling approach that optimizes design, guarantees the required high level of performance and takes into account the variability in the manufacturing process as well as the climatic variability in the use conditions. The efficiency of RBDO, however, depends on a solid understanding of the failure mechanisms caused by aging.

Creating a model of a dynamic system often involves developing a simplified model of its behavior based on realistic hypotheses and on the key parameters that are required for its functioning. The dynamic behavior of this modeled system is ruled by partial differential equations (PDEs). The model is then improved by introducing elements or parameters that were not initially included and by improving the set of PDEs (nonlinearity, coupling, etc.), in order to obtain a model that closely represents the reality of operating systems and provides pertinent simulation results.

The theoretical models that are based on the fundamental laws of physics use a bottom-up approach. These models can be studied using analytical or numerical methods. When experiments can be implemented, simulation results are compared to experimental results. It is also possible to use experimental methods and a top-down approach to build a database of the response of the system to applied stresses. These data are then analyzed by comparing them to the response of theoretical or empirical models. In all the cases, there is a degree of uncertainty in the statistical analysis of the data, which leads to predictions with a margin of error. The lower the margin of error, the closer the predictions are to reality, leading to a sound understanding of the functionalities of working materials.

As Book 9 of the “Reliability of Multiphysical Systems Set”, this book is designed to provide applications for Book 2 in the set, entitled Nanometer-scale Defect Detection Using Polarized Light. This is achieved by describing the experimental and theoretical methods developed in fundamental research laboratories to understand the physics or chemical processes, which at the nanometer scale are at the origin of the remarkable properties of the materials introduced in innovative technological devices. It presents optical techniques based on polarized light, which are used to characterize interface and bulk material defects that have an impact on the performance of nanodevices. It also describes how mechanical properties of nanomaterials can be determined using theoretical models and by the analysis of experimental results and their uncertainties.

This book is intended for students at master and doctoral levels, teaching academics and researchers in materials science, physics engineering and experimental study, as well as R&D and manufacturing engineers of large groups and SMEs in the field of electronics, mechatronics, or optical or electronic materials.

Chapter 1 provides a historical overview of the development of nanosciences and nanotechnologies and describes the challenges encountered when working on the nanometric scale, such as finding new ways to measure the physical properties of nanomaterials. It provides an overview of the techniques used for manufacturing nanomaterials: spin coating, cathode sputtering and laser ablation. Four characterization and failure analysis techniques adapted to nanotechnologies are presented: transmission electron microscopy (TEM), scanning electron microscopy (SEM), atomic force microscopy (AFM) and attenuated total reflection (ATR) infrared spectroscopy.

Chapter 2 describes how to manage system variable uncertainties in the design process. The objective is to obtain a design that meets the performance requirements, has a stable response when design parameters vary randomly and respects a threshold of minimal performance for a given confidence level. Several methods for analyzing the effect on the output of uncertainties in the system input parameters are presented with practical applications: a probabilistic approach, interval analysis, a fuzzy logic method, designs of experiments and principal component analysis.

Chapter 3 is dedicated to various applications of electromagnetic waves. After a quick summary of the main characteristics of electromagnetic waves and microwave antenna theory, the following applications are studied: energy of a monochromatic plane wave, properties of a rectangular waveguide, performance of a wire antenna and antenna networks. These applications facilitate the understanding of the operation of antennas for the fifth generation (5G) of mobile telecommunication systems.

Chapter 4 deals with functional materials employed in intelligent systems. The main characteristic of these intelligent materials is the coupling of their various physical properties. Thermodynamic coupling and multiphysics coupling are studied for piezoelectric, magnetostrictive and shape memory materials. Application exercises are provided for the deformations of a plate-like thin layer, a piezoelectric accelerometer, a piezoelectric transducer and a piezoelectric sensor.

Pierre Richard DAHOO

Philippe POUGNET

Abdelkhalak EL HAMI

October 2020