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This volume contains a collection of 19 papers from the 11th International Symposium on Ceramic Materials and Components for Energy and Environmental Applications (CMCEE-11), June 14-19, 2015 in Vancouver, BC, Canada. Papers were presented in the below five symposia from Track 2 on the topic of Ceramics for Energy Conservation and Efficiency: * Advanced Ceramics and Composites for Gas Turbine Engines * Advanced Refractory Ceramic Materials and Technologies * Advanced Ceramic Coatings for Power Systems * Energy Efficient Advanced Bearings and Wear Resistant Materials * Advanced Nitrides and Related Materials for Energy Applications

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Advanced and Refractory Ceramics for Energy Conservation and Efficiency

Ceramic Transactions, Volume 256A Collection of Papers Presented at CMCEE-11, June 14–19, 2015, Vancouver, BC, Canada

Edited by Hua-Tay Lin James HemrickVolume Editors Mrityunjay Singh Tatsuki Ohji Alexander Michaelis

Copyright © 2016 by The American Ceramic Society. All rights reserved.

Published by John Wiley & Sons, Inc., Hoboken, New Jersey.Published simultaneously in Canada.

No part of this publication may be reproduced, stored in a retrieval system, or transmitted in any form or by any means, electronic, mechanical, photocopying, recording, scanning, or otherwise, except as permitted under Section 107 or 108 of the 1976 United States Copyright Act, without either the prior written permission of the Publisher, or authorization through payment of the appropriate per-copy fee to the Copyright Clearance Center, Inc., 222 Rosewood Drive, Danvers, MA 01923, (978) 750-8400, fax (978) 750-4470, or on the web at www.copyright.com. Requests to the Publisher for permission should be addressed to the Permissions Department, John Wiley & Sons, Inc., 111 River Street, Hoboken, NJ 07030, (201) 748-6011, fax (201) 748-6008, or online at http://www.wiley.com/go/permission.

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Library of Congress Cataloging-in-Publication Data is available.

ISBN: 978-1-119-23458-6ISSN: 1042-1122

CONTENTS

Preface

Advanced Ceramics and Composites for Gas Turbine Engines

DAMAGE OF CERAMIC MATRIX COMPOSITES (CMCs) DURING MACHINING OPERATIONS

ABSTRACT

INTRODUCTION

EXPERIMENTAL

EVALUATION WITH FOCUS VARIATION AND IMAGE PROCESSING

RESULTS

CONCLUSION

ACKNOWLEDGEMENT

LITERATURE

CMCS: THE KEY FOR AFFORDABLE ACCESS TO SPACE

ABSTRACT

INTRODUCTION

CMCS FOR SSTO ENGINE APPLICATION

MECHANICAL PROPERTIES TESTING FOR ESCAPE DYNAMICS SPECIMENS

DISCUSSION

CONCLUSIONS

REFERENCES

NUMERICAL DETERMINATION OF EFFECTS OF TEMPERATURE ON INFILTRATION DYNAMICS OF LIQUID-COPPER AND TITANIUM/SOLID-CARBON SYSTEM

ABSTRACT:

INTRODUCTION

NUMERICAL PROCEDURE

RESULTS AND DISCUSSION

CONCLUSIONS

REFERENCES

OXIDATION AND HIGH TEMPERATURE RESISTANCE OF SiC/SiC COMPOSITES BY NITE-METHOD

ABSTRACT

INTRODUCTION

NITE PROCESS FOR SiC/SiC COMPOSITE FABRICATION

EXPERIMENTAL PROCEDURE

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGEMENTS

REFERENCES

HIGH PERFORMANCE SiC/SiC COMPONENT BY NITE-METHOD AND ITS APPLICATION TO ENERGY AND ENVIRONMENT

ABSTRACT

INTRODUCTION

RECENT EFFORTS ON HEAT RESISTANT SiC/SiC R & D

CYCLIC WATER QUENCHING TEST (CWQT)

CONCLUSIONS

ACKNOWLEDGEMENTS

REFERENCES

CERAMIC MATRIX COMPOSITES: CONCURRENT DEVELOPMENT OF MATERIALS AND CHARACTERIZATION TOOLS

ABSTRACT

INTRODUCTION

BACKGROUND

THROUGH THICKNESS MODULUS

NONDESTRUCTIVE ANALYSIS

FUTURE WORK

ACKNOWLEDGMENTS

REFERENCES

FABRICATION OF EBC SYSTEM WITH OXIDE EUTECTIC STRUCTURE

ABSTRACT

INTRODUCTION

EXPERIMENT

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGMENT

REFERENCES

Advanced Refractory Ceramic Materials and Technologies

THE USE OF ADVANCED CERAMIC MATERIALS IN OIL AND GAS APPLICATIONS

ABSTRACT

INTRODUCTION

CARBON-GRAPHITE MATERIALS FOR SEAL AND BEARING APPLICATIONS

CERAMIC MATERIALS FOR USE IN EROSIVE ENVIRONMENTS

CONCLUSION

REFERENCES

MICROSTRUCTURE AND ELASTIC PROPERTIES OF HIGHLY POROUS MULLITE CERAMICS PREPARED WITH WHEAT FLOUR

ABSTRACT

INTRODUCTION

THEORETICAL

EXPERIMENTAL

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGEMENT

REFERENCES

THE USE OF ADVANCED REFRACTORY CERAMIC MATERIALS TO ADDRESS INDUSTRIAL ENERGY EFFICIENCY CHALLENGES

ABSTRACT

INTRODUCTION

DISCUSSION

CONCLUSION

ACKNOWLEDGEMENTS

REFERENCES

AN APPROACH FOR MODELING SLAG CORROSION OF LIGHTWEIGHT Al

2

O

3

-MgO CASTABLES IN REFINING LADLE

ABSTRACT

INTRODUCTION

MATHEMATICAL MODEL

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGEMENT

REFERENCES

MICROSTRUCTURE, ELASTIC PROPERTIES AND HIGH-TEMPERATURE BEHAVIOR OF SILICA REFRACTORIES

ABSTRACT

INTRODUCTION

PHASE COMPOSITION AND ELASTIC PROPERTIES OF SILICA MATERIALS

EXPERIMENTAL

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGEMENT

REFERENCES

CEMENT FREE MAGNESIA BASED CASTABLES VERSUS MAGNESIA-SPINEL BRICKS IN CEMENT ROTARY KILNS

ABSTRACT

INTRODUCTION

PART I – THERMO-MECHANICAL BEHAVIOR

EXPERIMENTAL SET UP

RESULTS AFTER PREFIRING

RESULTS AFTER THERMAL SHOCK TEST

INTERMEDIATE CONCLUSION PART I

PART II – COMPARED INTRISIC PROPERTIES LINKED TO THERMO-CHEMICAL REQUIREMENTS

EXPERIMENTAL SET UP

EXPERIMENTAL RESULTS

CONCLUSION AND PERSPECTIVES

REFERENCES

EVALUATION OF REOXIDATION TENDENCY OF REFRACTORY MATERIALS IN STEEL METALLURGY BY A NEW TEST METHOD BASED ON CARRIER GAS HOT EXTRACTION

ABSTRACT

INTRODUCTION

METHODS AND MATERIALS

RESULTS Thermodynamic

DISCUSSION

OUTLOOK

ACKNOWLEDGMENT

REFERENCES

CERAMIC AND METAL-CERAMIC COMPONENTS WITH GRADED MICROSTRUCTURE

ABSTRACT

INTRODUCTION

EXPERIMENTAL PROCEDURES

RESULTS AND DISCUSSION

CONCLUSION

ACKNOWLEDGEMENT

REFERENCES

Energy Efficient Wear Resistant Materials

HIGH SPEED FORMATION OF FINE CERAMIC LAYERS BY NANOPARTICLES FILLER ROD THERMAL SPRAYING

ABSTRACT

INTRODUCTION

EXPERIMENTAL PROCEDURE

RESULTS AND DISCUSSION

CONCLUSIONS

REFERENCES

DEVELOPMENT OF SILICON NITRIDE BEARING COMPONENTS BY POWDER INJECTION MOLDING USING A NOVEL BINDER SYSTEM

ABSTRACT

INTRODUCTION

EXPERIMENTAL PROCEDURE

RESULTS & DISCUSSION

TOOL DESIGN

INJECTION MOULDING

INJECTION PRESSURE

INJECTION TEMPERATURE

OTHER PARAMETERS

TEST PART REPRODUCIBILITY

DESIGN OF THE DEBINDING PROCESS

THE SINTERING PROCESS

CONCLUSIONS

ACKNOWLEDGEMENT

REFERENCES

Advanced Coatings

STABILITY OF α-ALUMINA PHOTONIC STRUCTURES FORMED AT LOW TEMPERATURES UTILIZING CHROMIA-SEEDING

ABSTRACT

INTRODUCTION

EXPERIMENTAL

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGEMENTS

REFERENCES

POLYMER DERIVED GLASS CERAMIC LAYERS FOR CORROSION PROTECTION OF METALS

ABSTRACT

INTRODUCTION

EXPERIMENTAL

RESULTS AND DISCUSSION

CONCLUSIONS

ACKNOWLEDGMENTS

REFERENCES

Author Index

EULA

List of Tables

Chapter 1

Tab. 1

Chapter 2

Table I:

Chapter 3

Table I.

Chapter 6

Table I.

Chapter 8

Table I:

Table II:

Table III:

Table IV:

Chapter 9

Table 1:

Chapter 11

Table I.

Chapter 12

Table 1:

Table 2:

Table 3:

Chapter 13

Table I:

Table 2:

Chapter 14

Table 1:

Table 2:

Table 3:

Table 4:

Table 5:

Table 6:

Chapter 19

Tab. I:

Tab. II:

Tab. III:

Guide

Cover

Table of Contents

Preface

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Preface

The global challenges we face require innovative thinking and sustainable technology to meet increased demands for energy, clean water, and infrastructure. Research of materials, specifically ceramic materials, continues to provide solutions to everyday challenges such as environmental protection, energy supply and generation, and healthcare. The 11th International Symposium on Ceramic Materials and Components for Energy and Environmental Applications (11th CMCEE), held June 14–19, 2015 at the Hyatt Regency Vancouver in Vancouver, B.C., Canada, identified key challenges and opportunities for ceramic technologies to create sustainable development.

This Ceramic Transactions volume contains papers submitted from the following five symposia held in Track 2: Ceramics for Energy Conservation and Efficiency:

Advanced Ceramics and Composites for Gas Turbine Engines

Advanced Refractory Ceramic Materials and Technologies

Advanced Ceramic Coatings for Power Systems

Energy Efficient Advanced Bearings and Wear Resistant Materials

Advanced Nitrides and Related Materials for Energy Applications

After a peer-review process, 19 papers were accepted for inclusion in this proceedings volume. The editors wish to extend their gratitude and appreciation to all the symposium co-organizers for their help and support, to all the authors for their cooperation and contributions, to all the participants and session chairs for their time and efforts, and to all the reviewers for their valuable comments and suggestions. We also acknowledge the organization and leadership provided by the meeting chairs, Mrityunjay Singh, Tatsuki Ohji and Alexander Michaelis.

We hope that this proceedings will serve as a useful resource for the researchers and technologists in the field of energy conservation.

HUA-TAY LIN, Guangdong University of Technology, China

JAMES HEMRICK, Reno Refractories, Inc., USA

Advanced Ceramics and Composites for Gas Turbine Engines

CMCS: THE KEY FOR AFFORDABLE ACCESS TO SPACE

Johannes Petursson, Luis Gonzalez

Embry-Riddle Aeronautical University Daytona Beach, FL, 32114.

ABSTRACT

Escape Dynamics is designing a reusable single-stage-to-orbit launch system for small to medium payloads that would significantly lower the cost and turnaround times for accessing space. Part of the necessary increase in propulsion efficiency is a proprietary, innovative system where the energy is delivered to the moving vehicle by microwaves antennas on the ground, reducing the launcher weight dramatically. The microwave energy is converted into propulsive energy in Ceramic Matrix Composite heat exchangers.

A top level description of the system and the first step in the generation of design data is presented. Specifically, the elastic modulus and ultimate tensile strength. These mechanical properties were measured using specimens prepared following the ASTM standard. The test results are presented and discussed in the context of the intended application. Areas of further research and development are presented.

INTRODUCTION

To place a pound of payload in Earth orbit costs $10,000 (roughly $20,000/kg)1