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Advances in Industrial Mixing is a companion volume and update to the Handbook of Industrial Mixing. The second volume fills in gaps for a number of industries that were not covered in the first edition. Significant changes in five of the fundamental areas are covered in entirely updated or new chapters. The original text is provided as a searchable pdf file on the accompanying USB. * This book explains industrial mixers and mixing problems clearly and concisely. * Gives practical insights by the top professionals in the field, combining industrial design standards with fundamental insight. * Details applications in 14 key industries. Six of these are new since the first edition. * Provides the professional with information he/she did not receive in school. * Five completely rewritten chapters on mixing fundamentals where significant advances have happened since the first edition and seven concise update chapters which summarize critical technical information.
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Seitenzahl: 1582
Veröffentlichungsjahr: 2015
Edited bySuzanne M. KrestaProfessorUniversity of AlbertaEdmonton, CanadaArthur W. Etchells IIIDuPont Fellow Emeritus, Adjunct Professor Chemical Engineering, Rowan University, Glassboro, NJDavid S. DickeyMixTech, Inc., Coppell, Texas, USAVictor A. Atiemo-ObengFellow, Core Research & DevelopmentThe Dow Chemical Company (Retired), Midland, MI
Sponsored by the North American Mixing Forum
Cover: The dual cavern image is courtesy of Clara Gomez and Scott Webster, of Coanda Research & Development Corporation, Burnaby, BC, Canada.
Copyright © 2016 by John Wiley & Sons, Inc. All rights reserved
Published by John Wiley & Sons, Inc., Hoboken, New Jersey Published simultaneously in Canada.
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Library of Congress Cataloging-in-Publication Data is available.
ISBN: 978-0-470-52382-7
Contributors List
Editors’ Introduction
1 Organization of the Advances Volume
2 Mixing in Perspective
3 Scope of the
HANDBOOK
and
ADVANCES VOLUME
4 Mixing Nomenclature and Unit Conversions
5 Acknowledgments
References
Contents of the DVD, Including Instructional Videos
Electronic (PDF) Version of the Handbook of Industrial Mixing
Color Figures and Troubleshooting Charts
22 Instructional Videos
Video Library
Sources of Additional Videos
Introduction: A Technical Definition of Mixing
Range of Industrial Mixing Applications
Three Dimensions of Segregation: A Technical Definition of Mixing
Identifying Mixing Problems: Defining the Critical Scales and Process Objectives
Notation
References
Chapter 1a Residence Time Distributions
1a-1 Introduction
Chapter 1b Mean Age Theory for Quantitative Mixing Analysis
1b-1 Introduction
1b-2 Age and Time in a Flow System
1b-3 Governing Equations of Mean Age and Higher Moments
1b-4 Computation of Mean Age
1b-5 Relations of Mean Age and Residence Time Distribution
1b-6 Variances and the Degree of Mixing
1b-7 Mean Age and Concentration in a CFSTR
1b-8 Probability Distribution Function of Mean Age
1b-9 Future Development of Mean Age Theory
Nomenclature
References
Chapter 2a Turbulence in Mixing Applications
2a-1 Introduction
Chapter 2b Update to Turbulence in Mixing Applications
2b-1 Introduction
2b-2 The Velocity Field and Turbulence
2b-3 Spectrum of Turbulent Length Scales: Injection of Scalar (Either Reagent or Additive) and the Macro-, Meso-, and Microscales of Mixing
2b-4 Turbulence and Mixing of Solids, Liquids, and Gases
2b-5 Specifying Mixing Requirements for a Process
2b-6 Conclusions
Notation
References
Chapter 3a Laminar Mixing: A Dynamical Systems Approach
3a-1 Introduction
Chapter 3b Microstructure, Rheology, and Processing of Complex Fluids
3b-1 Introduction
3b-2 Literature Analysis—Mixing of Complex Fluids
3b-3 Common Complex Fluid Rheology Classes and Their Effects
3b-4 Conclusions
Nomenclature
Notes
References
Chapter 4 Experimental Methods:
4-1 Introduction
Chapter 5a Computational Fluid Mixing
5a-1 Introduction
Chapter 5b CFD Modeling of Stirred Tank Reactors
5b-1 Numerical Issues
5b-2 Turbulence Models
5b-3 Quantitative Predictions
5b-4 Modeling Other Physics
Nomenclature
References
Chapter 6a Mechanically Stirred Vessels
6b-1 Introduction
Chapter 6b Flow Patterns and Mixing
6b-1 Introduction
6b-2 Circulation Patterns
6b-3 Coupling the Velocity Field with Applications
Nomenclature
References
Chapter 6c Vessel Heads: Depths, Volumes, and Areas
6c-1 Head Depth
6c-2 Head Volume
6c-3 Head Area
6c-4 Dimensionless Coefficients for Torispherical Heads
6c-5 Calculations for Conical Bottoms
6c-6 Other Types of Bottoms
Nomenclature
References
Chapter 7a Mixing in Pipelines
7a-1 Introduction
Chapter 7b Update to Mixing in Pipelines
7b-1 Introduction
7b-2 Use of CFD with Static Mixers
7b-3 Recent Developments in Single-Phase Blending
7b-4 Recent Developments in Multiphase Dispersions
7b-5 Mixing with Static Mixers When Solids Are Present
Notation
Bibliography
References
Chapter 7c Introduction to Micromixers
7c-1 Introduction
7c-2 Mixing and Transport Phenomena
7c-3 Micromixer Geometries and Fluid Contacting Mechanisms
7c-4 Characterization of Flow and Mixing
7c-5 Multiphase Mixing
7c-6 Commercial Equipment and Industrial Examples
7c-7 Evaluation of the Current and Future Applicability of Microreactors in Industry
Notation
Suggested Reading
References
Chapter 8 Rotor–Stator Mixing Devices
8.1 Introduction
Chapter 9a Blending of Miscible Liquids
9.1 Introduction
Chapter 9b Laminar Mixing Processes in Stirred Vessels
9b-1 Introduction
9b-2 Laminar Mixing Background
9b-3 Rheologically complex fluids
9b-4 Heat Effects
9b-5 Laminar Mixing Equipment
9b-6 Key Design Parameters
9b-7 Power Number and Power Constant
9b-8 Experimental Techniques to Determine Blend Time
9b-9 Mixing Efficiency
9b-10 Characterization of the Mixing Flow Field
9b-11 Hydrodynamic Characterization of Laminar Blending
9b-12 Application of Chaos in Mixing
9b-13 Selecting an Appropriate Geometry for Generic Applications
9b-14 Heat and Mass Transfer in the Laminar Mixing
9b-15 Industrial Mixing Process Requirements
9b-16 Scale-up Rules in the Laminar Regime
9b-17 Mixer Troubleshooting and Engineering Calculations
9b-18 Concluding Remarks
Acknowledgments
References
Chapter 10 Solid–Liquid Mixing
10-1 Introduction and Scope
10-2 Solid and Liquid Physical Characteristics
10-3 Agitation of Sinking or Settling Solids
10-4 Incorporation and Dispersion of Floating Solids (N. G. Özcan-Taşkin)
10-5 Attrition and Particle Damage
10-6 Solids Suspension and Distribution Using Liquid Jets
10-7 Mass Transfer
10-8 Lab and Pilot-Scale Testing
Nomenclature
References
Chapter 11 Gas—Liquid Mixing in Turbulent Systems
11-1 Introduction
Chapter 12 Immiscible Liquid–Liquid Systems
12-1 Introduction
Chapter 13a Mixing and Chemical Reactions
13a-1 Introduction
Chapter 13b Scale-up Using the Bourne Protocol: Reactive Crystallization and Mixing Example
13b-1 Example: Redesigning an Uncontrolled Precipitation to a Reactive Crystallization
Notes
References
Chapter 14a Heat Transfer
14a-1 Introduction
Chapter 14b Heat Transfer In Stirred Tanks—Update
14b-1 Introduction
14b-2 Consideration of Heat Transfer Surfaces used in Mixing Systems
14b-3 Heating And Cooling Of Liquids
14b-4 Summary of Proposed Equations Used in Heat Transfer for Stirred Tanks
14b-5 Methodology for Design of Heating for a Mixing System
14b-6 Example
Acknowledgments
Notes
References
Chapter 15 Solids Mixing
15-1 Introduction: Fundamentals of Solids Mixing
15-2 Introduction: Industrial Applications
Chapter 16 Mixing of Highly Viscous Fluids, Polymers, and Pastes
16-1 Introduction
Chapter 17 Mixing in the Fine Chemicals and Pharmaceutical Industries
17-1 Introduction
Chapter 18 Mixing in the Fermentation and Cell Culture Industries
18-1 Introduction
Chapter 19 Fluid Mixing Technology in the Petroleum Industry
19.1 Introduction
Chapter 20 Mixing in the Pulp and Paper Industry
20-1 Introduction
Chapter 21a Mechanical Design of Mixing Equipment
21a-1 Introduction
Chapter 21b Magnetic Drives for Mixers
21b-1 Introduction
21b-2 Laboratory Magnetic Stirrers
21b-3 Top-Entering Magnetic Mixer Drives
21b-4 Bottom-Entering Magnetic Mixer Drives
Chapter 22 Role of the Mixing Equipment Supplier
22-1 Introduction
Chapter 23 Commissioning Mixing Equipment
23-1 Introduction
23-2 Commissioning Concepts
23-3 Instructions for Commissioning
23-4 Safety Instructions
23-5 Receiving the Equipment
23-6 Kinds of Storage
23-7 Installation
23-8 Lubrication
23-9 Wiring
23-10 Initial Operation
23-11 Troubleshooting
23-12 Maintenance
23-13 Commissioning Shaft Seals
23-14 Mechanical Checkout, Startup, and Troubleshooting of Agitator Equipment
23-15 Summary
Nomenclature
References
Chapter 24 Mixing Safety
24-1 Introduction
24-2 The Practice of Risk Management
24-3 Summary Comments on Mixing Safety
References
Chapter 25 Mixing Issues in Crystallization and Precipitation Operations
25-1 Introduction
25-2 Basic Crystallization Concepts
25-3 Impact of Mixing on Primary Heterogeneous Nucleation
25-4 Impact of Mixing on Secondary Nucleation
25-5 Impact of Mixing on Crystal Growth and Dissolution Rates
25-6 Selecting Operating Conditions to Optimize Crystal Suspension and Withdrawal
25-7 Damkoehler Number for Nucleation and Subsurface Feeding of Reactants
25-8 Stirred Vessel Crystallizers
25-9 Other Types of Equipment
25-10 Precipitation
25-11 Agglomeration and Oiling Out
25-12 Conclusions
Nomenclature
References
Appendices
Chapter 26 Mixing in the Water and Wastewater Industry
26-1 Introduction
26-2 Mixing in Drinking Water Treatment
26-3 Mixing in Wastewater Treatment
26-4 Mixing in Sludge Treatment
26-5 Conclusions
Nomenclature
References
Chapter 27 Mixing in the Food Industry
27-1 Introduction
27-2 Building or Reducing Texture Through Mixing
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