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Beschreibung

This book provides an up-to-date overview of the methods, hardware and approaches in magnetic resonance microscopy. A wide range of applications are discussed in material science and engineering, life sciences and electrochemical systems.

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Veröffentlichungsjahr: 2022

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Magnetic Resonance Microscopy

Instrumentation and Applications in Engineering, Life Science, and Energy Research

Edited by

 

Sabina Haber-Pohlmeier

Aachen

 

Bernhard Blümich

Aachen

 

Luisa Ciobanu

Paris

 

 

Editors

Sabina Haber-PohlmeierRWTH Aachen UniversityWorringerweg 252074 AachenGermany

Bernhard BlümichRWTH Aachen UniversityWorringerweg 252074 AachenGermany

Luisa CiobanuNeuroSpin, CEA-SaclayBat 145, Point Courrier 15691191 Gif sur Yvette France France

Cover Image: Courtesy of Denis Wypysek, Jan Korvink, Henk Van As, and Luisa Ciobanu

All books published by WILEY-VCH are carefully produced. Nevertheless, authors, editors, and publisher do not warrant the information contained in these books, including this book, to be free of errors. Readers are advised to keep in mind that statements, data, illustrations, procedural details or other items may inadvertently be inaccurate.

Library of Congress Card No.:

Names: Haber-Pohlmeier, Sabina, 1962- editor. | Blümich,Bernhard, editor. | Ciobanu, Luisa, editor.Title: Magnetic resonance microscopy : instrumentation and applications in engineering, life science and energy research / edited by Sabina Haber-Pohlmeier, Bernhard Blümich, Luisa Ciobanu.Description: Hoboken, New Jersey : John Wiley & Sons, [2022] | Includes bibliographical references and index.Identifiers: LCCN 2021061399 (print) | LCCN 2021061400 (ebook) | ISBN 9783527347605 (hardback) | ISBN 9783527827237 (pdf) | ISBN 9783527827251 (epub) | ISBN 9783527827244 (ebook)Subjects: LCSH: Magnetic resonance microscopy. | Magnetic resonance microscopy—Industrial applications.Classification: LCC QC762.6.M34 M344 2022 (print) | LCC QC762.6.M34 (ebook) | DDC 502.8/2--dc23/eng20220215LC record available at https://lccn.loc.gov/2021061399LC ebook record available at https://lccn.loc.gov/2021061400

British Library Cataloguing-in-Publication DataA catalogue record for this book is available from the British Library.

Bibliographic information published by the Deutsche NationalbibliothekThe Deutsche Nationalbibliothek lists this publication in the Deutsche Nationalbibliografie; detailed bibliographic data are available on the Internet at http://dnb.d-nb.de.

© 2022 Wiley-VCH GmbH, Boschstraße 12, 69469Weinheim, Germany

All rights reserved (including those of translation into other languages). No part of this book may be reproduced in any form – by photoprinting, microfilm, or any other means – nor transmitted or translated into a machine language without written permission from the publishers. Registered names, trademarks, etc. used in this book, even when not specifically marked as such, are not to be considered unprotected by law.

Print ISBN: 978-3-527-34760-5ePDF ISBN: 978-3-527-82723-7ePub ISBN: 978-3-527-82725-1oBook ISBN: 978-3-527-82724-4

Cover Design: Wiley

Typesetting: Set in 9.5/12.5pt STIXTwoText by Integra Software Services Pvt. Ltd, Pondicherry, IndiaPrinting and Binding: Bell & Bain

Printed on acid-free paper

Contents

Cover

Title page

Copyright

Foreword

Preface

Part I: Developments in Hardware and Methods

1 Microengineering Improves MR Sensitivity: Neil MacKinnon, Jan G. Korvink, and Mazin Jouda

2 Ceramic Coils for MR Microscopy: Marine A.C. Moussu, Redha Abdeddaim, Stanislav Glybovski, Stefan Enoch, and Luisa Ciobanu

3 Portable Brain Scanner Technology for Use in Emergency Medicine: Lawrence L. Wald and Clarissa Z. Cooley

4 Technology for Ultrahigh Field Imaging: Kamil Uğurbil

5 Sweep Imaging with Fourier Transformation (SWIFT): Djaudat Idiyatullin and Michael Garwood

6 Methods Based on Solution Flow, Improved Detection, and Hyperpolarization for Enhanced Magnetic Resonance: Patrick Berthault and Gaspard Huber

7 Advances and Adventures with Mobile NMR: Bernhard Blümich, Denis Jaschtschuk, and Christian Rehorn

Part II: Applications in Chemical Engineering

8 Ultrafast MR Techniques to Image Multi-phase Flows in Pipes and Reactors: Bubble Burst Hydrodynamics Andrew J. Sederman, Andi Reci, and Lynn F. Gladden

9 Magnetic Resonance Imaging of Membrane Filtration Processes Denis Wypysek and Matthias Wessling

10 Whither NMR of Biofilms? Joseph D. Seymour, Gisela Guthausen, and Catherine M. Kirkland

11 MRI of Transport and Flow in Plants and Foods Maria Raquel Serial, Camilla Terenzi, John van Duynhoven, and Henk Van As

Part III: Applications in Life Sciences

12 MRI of Single Cells Labeled with Superparamagnetic Iron Oxide Nanoparticles: Cornelius Faber

13 Imaging Biomarkers for Alzheimer’s Disease Using Magnetic Resonance Microscopy: Alexandra Badea, Jacques A. Stout, Robert J. Anderson, Gary P. Cofer, Leo L. Duan, and Joshua T. Vogelstein

14 NMR Imaging of Slow Flows in the Root–Soil Compartment: Sabina Haber-Pohlmeier, Petrik Galvosas, Jie Wang, and Andreas Pohlmeier

15 Magnetic Resonance Studies of Water in Wood Materials: Bruce J. Balcom and Minghui Zhang

Part IV: Applications in Energy Research

16 In Situ Spectroscopic Imaging of Devices for Electrochemical Storage with Focus on the Solid Components: Elodie Salager

17 Magnetic Field Map Measurements and Operando NMR/MRI as a Diagnostic Tool for the Battery Condition: Stefan Benders and Alexej Jerschow

18 Magnetic Resonance Imaging of Sodium-Ion Batteries: Claire L. Doswell, Galina E. Pavlovskaya, Thomas Meersmann, and Melanie M. Britton

19 The Fun of Applications – a Perspective: Y.-Q. Song

Index

End User License Agreement

List of Tables

Chapter 2

Table 2.1 Literature review of dielectric probes for MRI.

Chapter 4

Table 4.1 Preliminary data on the ratio...

Chapter 11

Table 11.1 Overview of the past...

Table 11.2 Overview of the past...

Chapter 12

Table 12.1 Types of iron oxide nanoparticle by size.

Guide

Cover

Title page

Copyright

Table of Contents

Foreword

Preface

Begin Reading

Index

End User License Agreement

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Foreword

This book is the fourth in the Wiley-VCH series on Magnetic Resonance Microscopy, a series linked in spirit to the International Conference on Magnetic Resonance Microscopy (ICMRM). Winfried Kuhn and Bernhard Blümich organized the first meeting of this biannual conference in 1991 in Heidelberg, which led to the first book in this series. That Heidelberg meeting is also when Paul Callaghan burst upon the scene (with his student Yang Xia, who remains active in these meetings) with his new, but now classic, book Principles of Nuclear Magnetic Resonance Microscopy (Oxford University Press) – what timing! The wider appearance of magnetic gradient fields in the portfolio of magnetic resonance methods for imaging and studies of molecular transport phenomena was an exciting prospect. It motivated the still ongoing ICMRM conference series and the associated books, which summarize the progress in this field with chapters written by leading experts, among them Nobel Prize awardees Paul Lauterbur and Sir Peter Mansfield as well as Sir Paul Callaghan, who shaped that community like a force of nature from then on until his untimely death in 2012. Also, our brilliant colleague Robert Blinc from Slovenia attended the first ICMRM but had to leave early following an announcement during one of the sessions effectively saying “Professor Blinc, you are needed back in your country,” at which Robert Blinc stood up and left to facilitate the independence of Slovenia from Socialist Federal Republic of Yugoslavia. We were witnessing the birth of a country, a unique experience for most of us. At the third meeting in Würzburg, the brave suggestion to hold a meeting in North America was accepted. Thus, the fourth meeting was in Albuquerque and ICMRM has now a truly international presence, having ventured as far away as Utsunomiya and Beijing. These meetings, originally dubbed the Heidelberg Meetings, have been at the forefront of amazing developments and accompanying applications of magnetic resonance. Despite the inclusion of the word microscopy in their name, they represent the much broader area of magnetic resonance with spatial resolution, which is expressed by the title of the second book from the Albuquerque meeting, Spatially Resolved Magnetic Resonance, as well as the organizing Division of Spatially Resolved Magnetic Resonance of the AMPERE Society. Thanks to the advances over three decades, we have micrometer spatial resolution in magnetic resonance imaging today, while in the early days the word microscopy was understood as a tool to see things hard to visualize just by eye. We believe the broad range of the science and applications of magnetic resonance represented in these meetings is unique to all science and the field displays no hint of imminent stagnation – welcome news to all of us. I would like to close this Foreword with the observation that Bernhard Blümich, who with Winfried Kuhn founded these meetings 30 years ago, is still actively involved here as one of the editors of this book. I salute him for his continued contributions to the field and support of this conference.

Eiichi FukushimaAlbuquerque, 2021

Preface

Magnetic resonance microscopy (MRM) has focused on magnetic resonance imaging (MRI) applied to objects of smaller scale and higher spatial resolution for more than three decades. After the pioneering work by Eccles, Callaghan, Aguayo, Blackband, Johnson et al. in 1986, MRM quickly spread to, among other fields, chemistry, histology, and materials research. Since 1992, the edited book series Magnetic Resonance Microscopy has provided an important voice describing the latest developments in spatially resolved magnetic resonance methods and their applications far beyond the scope of medical diagnostics. An excellent introduction to MRM, focusing on the practical aspects of high magnetic fields and on the study of biological systems, was authored in 2017 by Luisa Ciobanu: Microscopic Magnetic Resonance Imaging: A Practical Perspective (Pan Stanford, Singapore, 2017). Our book complements this monograph by showing the use of MRM and related techniques in a much broader area and on a wider scale, which extends from chemical engineering to plant research and battery applications, highlighting the interdisciplinary nature of MRM.

The book opens with a section on hardware and methodology, covering aspects of micro-engineering, magnet technology, coil performance, and hyperpolarization to improve signal-to-noise ratio, a major bottleneck of MRM. Specific pulse sequences and developments in the field of mobile nuclear magnetic resonance are further topics of this first chapter. The following parts, 2 and 3, review essential processes such as filtration, multi-phase flows and transport, and a wide range of systems from biomarkers via single cells to plants and biofilms. Part 4 focuses on energy research, which is becoming increasingly important due to the globally growing environmental problems. It reports on battery types and their developments and how battery states can be recorded and characterized with MRM. However, we would like to point out that only a small number of applications could be addressed in this book. Finally, the last chapter advocates that theory and applications should not be treated separately, because much can be gained from their complementarity.

The main aim of this book is to convince aspiring and established scientists from all fields that MRM is a versatile nuclear magnetic resonance (NMR) method that is capable of answering many questions from both the laboratory and everyday life. The book seeks to inspire a new readership from industries and innovative research directions to create synergies by adding MRM to their expertise.

The editors thank all the authors for contributing their invaluable knowledge to this book during a time challenged by COVID-19. Our thanks also go to the kind staff of the Wiley books department, who helped us with advice and support throughout the whole editing process.

Sabina Haber-PohlmeierLuisa CiobanuBernhard BlümichSummer 2021

Part I Developments in Hardware and Methods