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Beschreibung

The book consists of a series of edited chapters, each written by an expert in the field and focusing on a particular characterization technique as applied to glass.  The book covers a variety of techniques ranging from the very common (like Raman and FTIR) to the most recent (and less well known) ones, like SEM for structural analysis and photoelastic measurements.  The level of the chapters make it suitable for researchers and for graduate students about to start their research work. It will also:

  • discuss the technique itself, background, nuances when it comes to looking at glassy materials, interpretation of results, case studies, and recent and near-future innovations
  • Fill a widening gap in modern techniques for glass characterization
  • Provide much needed updates on the multiple essential characterization techniques  

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Veröffentlichungsjahr: 2015

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MODERN GLASS CHARACTERIZATION

Edited by

Mario Affatigato

Copyright © 2015 by The American Ceramic Society and John Wiley & Sons, Inc. All rights reserved.

Published by John Wiley & Sons, Inc., Hoboken, New Jersey. Published simultaneously in Canada.

No part of this publication may be reproduced, stored in a retrieval system, or transmitted in any form or by any means, electronic, mechanical, photocopying, recording, scanning, or otherwise, except as permitted under Section 107 or 108 of the 1976 United States Copyright Act, without either the prior written permission of the Publisher, or authorization through payment of the appropriate per-copy fee to the Copyright Clearance Center, Inc., 222 Rosewood Drive, Danvers, MA 01923, (978) 750-8400, fax (978) 750-4470, or on the web at www.copyright.com. Requests to the Publisher for permission should be addressed to the Permissions Department, John Wiley & Sons, Inc., 111 River Street, Hoboken, NJ 07030, (201) 748-6011, fax (201) 748-6008, or online at http://www.wiley.com/go/permission.

Limit of Liability/Disclaimer of Warranty: While the publisher and author have used their best efforts in preparing this book, they make no representations or warranties with respect to the accuracy or completeness of the contents of this book and specifically disclaim any implied warranties of merchantability or fitness for a particular purpose. No warranty may be created or extended by sales representatives or written sales materials. The advice and strategies contained herein may not be suitable for your situation. You should consult with a professional where appropriate. Neither the publisher nor author shall be liable for any loss of profit or any other commercial damages, including but not limited to special, incidental, consequential, or other damages.

For general information on our other products and services or for technical support, please contact our Customer Care Department within the United States at (800) 762-2974, outside the United States at (317) 572-3993 or fax (317) 572-4002.

Wiley also publishes its books in a variety of electronic formats. Some content that appears in print may not be available in electronic formats. For more information about Wiley products, visit our web site at www.wiley.com.

Library of Congress Cataloging-in-Publication Data is available.

ISBN: 978-1-118-23086-2

CONTENTS

PREFACE

LIST OF CONTRIBUTORS

1 DENSITY, THERMAL PROPERTIES, AND THE GLASS TRANSITION TEMPERATURE OF GLASSES

Part I: Introduction to Physical Properties and Their Uses

Part II: Density

1.1 DENSITY: EXPERIMENTAL BACKGROUND AND THEORY

Part III: Thermal Effects with a Focus on the Glass Transition Temperature

1.2 OVERVIEW

1.3 EXPERIMENTAL METHODS AND THEORY

1.4 INSTRUMENTATION USED FOR DETERMINING

T

g

AND RELATED THERMAL EVENTS

1.5 ANALYSIS OF DATA AND EXTRACTION OF USEFUL INFORMATION

1.6 CASE STUDIES FROM GLASS SYSTEMS

1.7 CONCLUSION TO THERMAL PROPERTIES

ACKNOWLEDGMENTS

REFERENCES

2 INFRARED SPECTROSCOPY OF GLASSES

2.1 INTRODUCTION

2.2 BACKGROUND AND THEORY

2.3 INSTRUMENTATION

2.4 ANALYSIS OF INFRARED DATA

2.5 CASE STUDIES

2.6 CONCLUSIONS

ACKNOWLEDGMENTS

REFERENCES

3 RAMAN SPECTROSCOPY OF GLASSES

3.1 INTRODUCTION

3.2 BACKGROUND

3.3 INSTRUMENTATION AND DATA ANALYSIS

3.4 CASE STUDIES

3.5 CONCLUSIONS

ACKNOWLEDGMENTS

REFERENCES

4 BRILLOUIN LIGHT SCATTERING

4.1 INTRODUCTION

4.2 BACKGROUND AND THEORY

4.3 INSTRUMENTATION

4.4 DATA ANALYSIS AND INFORMATION CONTENT

4.5 EXAMPLES OF CASE STUDIES

4.6 SUMMARY

REFERENCES

5 NEUTRON DIFFRACTION TECHNIQUES FOR STRUCTURAL STUDIES OF GLASSES

5.1 INTRODUCTION

5.2 INSTRUMENTATION

5.3 THEORETICAL ASPECTS OF NEUTRON DIFFRACTION ON GLASSES

5.4 THE APPLICATION OF NEUTRON DIFFRACTION TO STUDIES OF GLASS STRUCTURE

ACKNOWLEDGMENTS

REFERENCES

FURTHER READING

Notes

6 X-RAY DIFFRACTION FROM GLASS

6.1 INTRODUCTION

6.2 BACKGROUND/THEORY

6.3 ANALYSIS OF DATA, EXTRACTION OF USEFUL INFORMATION

6.4 INSTRUMENTATION

6.5 CASE STUDIES

6.6 CONCLUSIONS

ACKNOWLEDGMENTS

REFERENCES

7 XAFS SPECTROSCOPY AND GLASS STRUCTURE

7.1 INTRODUCTION

7.2 THE ORIGINS OF X-RAY ABSORPTION SPECTRA

7.3 XAFS INSTRUMENTATION

7.4 THE PHYSICAL MECHANISM OF XAFS

7.5 EXAFS

7.6 XAFS DATA ANALYSIS

7.7 EXAFS ACCURACY AND LIMITATIONS

7.8 XANES

7.9 XAFS SPECTROSCOPY APPLIED TO GLASS STRUCTURE: SOME EXAMPLES

7.10 SUMMARY AND CONCLUSIONS

REFERENCES

8 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY OF GLASSES

8.1 INTRODUCTION

8.2 THEORETICAL BACKGROUND

8.3 INSTRUMENTATION

8.4 DATA ANALYSIS AND STRUCTURAL INTERPRETATION

8.5 CASE STUDIES

8.6 CONCLUSIONS

ACKNOWLEDGMENTS

REFERENCES

9 ADVANCED DIPOLAR SOLID STATE NMR SPECTROSCOPY OF GLASSES

9.1 INTRODUCTION

9.2 THEORETICAL ASPECTS

9.3 HETERONUCLEAR EXPERIMENTS

9.4 HOMONUCLEAR EXPERIMENTS

9.5 CASE STUDIES

ACKNOWLEDGMENTS

REFERENCES

10 ATOM PROBE TOMOGRAPHY OF GLASSES

10.1 INTRODUCTION

10.2 BACKGROUND AND THEORY

10.3 INSTRUMENTATION

10.4 ANALYSIS METHODS

10.5 CASE STUDIES

ACKNOWLEDGMENTS

REFERENCES

INDEX

EULA

List of Tables

Chapter 1

Table 1.1

Table 1.2

Table 1.3

Table 1.4

Table 1.5

Chapter 2

Table 2.1

Chapter 4

Table 4.1

Chapter 5

Table 5.1

Table 5.2

Table 5.3

Table 5.4

Table 5.5

Chapter 6

Table 6.1

Chapter 7

Table 7.1

Chapter 8

Table 8.1

Chapter 10

Table 10.1

Table 10.2

Guide

Cover

Table of Contents

Preface

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