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The book consists of a series of edited chapters, each written by an expert in the field and focusing on a particular characterization technique as applied to glass. The book covers a variety of techniques ranging from the very common (like Raman and FTIR) to the most recent (and less well known) ones, like SEM for structural analysis and photoelastic measurements. The level of the chapters make it suitable for researchers and for graduate students about to start their research work. It will also:
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Seitenzahl: 889
Veröffentlichungsjahr: 2015
Edited by
Mario Affatigato
Copyright © 2015 by The American Ceramic Society and John Wiley & Sons, Inc. All rights reserved.
Published by John Wiley & Sons, Inc., Hoboken, New Jersey. Published simultaneously in Canada.
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ISBN: 978-1-118-23086-2
PREFACE
LIST OF CONTRIBUTORS
1 DENSITY, THERMAL PROPERTIES, AND THE GLASS TRANSITION TEMPERATURE OF GLASSES
Part I: Introduction to Physical Properties and Their Uses
Part II: Density
1.1 DENSITY: EXPERIMENTAL BACKGROUND AND THEORY
Part III: Thermal Effects with a Focus on the Glass Transition Temperature
1.2 OVERVIEW
1.3 EXPERIMENTAL METHODS AND THEORY
1.4 INSTRUMENTATION USED FOR DETERMINING
T
g
AND RELATED THERMAL EVENTS
1.5 ANALYSIS OF DATA AND EXTRACTION OF USEFUL INFORMATION
1.6 CASE STUDIES FROM GLASS SYSTEMS
1.7 CONCLUSION TO THERMAL PROPERTIES
ACKNOWLEDGMENTS
REFERENCES
2 INFRARED SPECTROSCOPY OF GLASSES
2.1 INTRODUCTION
2.2 BACKGROUND AND THEORY
2.3 INSTRUMENTATION
2.4 ANALYSIS OF INFRARED DATA
2.5 CASE STUDIES
2.6 CONCLUSIONS
ACKNOWLEDGMENTS
REFERENCES
3 RAMAN SPECTROSCOPY OF GLASSES
3.1 INTRODUCTION
3.2 BACKGROUND
3.3 INSTRUMENTATION AND DATA ANALYSIS
3.4 CASE STUDIES
3.5 CONCLUSIONS
ACKNOWLEDGMENTS
REFERENCES
4 BRILLOUIN LIGHT SCATTERING
4.1 INTRODUCTION
4.2 BACKGROUND AND THEORY
4.3 INSTRUMENTATION
4.4 DATA ANALYSIS AND INFORMATION CONTENT
4.5 EXAMPLES OF CASE STUDIES
4.6 SUMMARY
REFERENCES
5 NEUTRON DIFFRACTION TECHNIQUES FOR STRUCTURAL STUDIES OF GLASSES
5.1 INTRODUCTION
5.2 INSTRUMENTATION
5.3 THEORETICAL ASPECTS OF NEUTRON DIFFRACTION ON GLASSES
5.4 THE APPLICATION OF NEUTRON DIFFRACTION TO STUDIES OF GLASS STRUCTURE
ACKNOWLEDGMENTS
REFERENCES
FURTHER READING
Notes
6 X-RAY DIFFRACTION FROM GLASS
6.1 INTRODUCTION
6.2 BACKGROUND/THEORY
6.3 ANALYSIS OF DATA, EXTRACTION OF USEFUL INFORMATION
6.4 INSTRUMENTATION
6.5 CASE STUDIES
6.6 CONCLUSIONS
ACKNOWLEDGMENTS
REFERENCES
7 XAFS SPECTROSCOPY AND GLASS STRUCTURE
7.1 INTRODUCTION
7.2 THE ORIGINS OF X-RAY ABSORPTION SPECTRA
7.3 XAFS INSTRUMENTATION
7.4 THE PHYSICAL MECHANISM OF XAFS
7.5 EXAFS
7.6 XAFS DATA ANALYSIS
7.7 EXAFS ACCURACY AND LIMITATIONS
7.8 XANES
7.9 XAFS SPECTROSCOPY APPLIED TO GLASS STRUCTURE: SOME EXAMPLES
7.10 SUMMARY AND CONCLUSIONS
REFERENCES
8 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY OF GLASSES
8.1 INTRODUCTION
8.2 THEORETICAL BACKGROUND
8.3 INSTRUMENTATION
8.4 DATA ANALYSIS AND STRUCTURAL INTERPRETATION
8.5 CASE STUDIES
8.6 CONCLUSIONS
ACKNOWLEDGMENTS
REFERENCES
9 ADVANCED DIPOLAR SOLID STATE NMR SPECTROSCOPY OF GLASSES
9.1 INTRODUCTION
9.2 THEORETICAL ASPECTS
9.3 HETERONUCLEAR EXPERIMENTS
9.4 HOMONUCLEAR EXPERIMENTS
9.5 CASE STUDIES
ACKNOWLEDGMENTS
REFERENCES
10 ATOM PROBE TOMOGRAPHY OF GLASSES
10.1 INTRODUCTION
10.2 BACKGROUND AND THEORY
10.3 INSTRUMENTATION
10.4 ANALYSIS METHODS
10.5 CASE STUDIES
ACKNOWLEDGMENTS
REFERENCES
INDEX
EULA
Chapter 1
Table 1.1
Table 1.2
Table 1.3
Table 1.4
Table 1.5
Chapter 2
Table 2.1
Chapter 4
Table 4.1
Chapter 5
Table 5.1
Table 5.2
Table 5.3
Table 5.4
Table 5.5
Chapter 6
Table 6.1
Chapter 7
Table 7.1
Chapter 8
Table 8.1
Chapter 10
Table 10.1
Table 10.2
Cover
Table of Contents
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